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Application note · Failure analysis

Parylene removal by oxygen plasma for failure analysis

Parylene conformal coatings protect PCBs, sensors, MEMS and medical implants because they resist almost every solvent — which is exactly why they are hard to remove for failure analysis or rework. Oxygen plasma removes parylene cleanly and tells you when it is done.

  • ≈230 nm/min at 150 W
  • Automatic end-point reading
  • Electrical contact restored
Glass slide coated with 4.7 micrometer parylene film showing rainbow interference pattern
Before: 4.67 µm parylene on glass (note interference colors)
Clear glass slide after 25 minutes of oxygen plasma, parylene completely removed
After 25 min O₂ plasma: film completely removed
Test 1

Parylene film on glass, 150 W direct mode

Customer-supplied glass slides coated on both sides with ≈4.67 µm parylene. Recipe 1: 150 W, 5 sccm O₂, 92 mTorr, direct (immersion) mode, run in 5-minute steps in a Tergeo plasma system.

Total timePlasma emission readingObservation
Empty chamber94Pure O₂ baseline
5 min≈210By-products (H₂O, COₓ) raise the reading; film still soft and scratchable
10 min≈210Two spots cleared
15 min205Top corner mostly cleared
20 min99Film mostly removed; surface can no longer be scratched
25 min91At baseline — film completely gone

Estimated etch rate ≈230 nm/min (4.67 µm in ≈20 min).

Parylene coated slide before etching
0 min: coated
Parylene coated slide after 10 minutes of oxygen plasma with two cleared spots
10 min: first spots clear
Slide after 20 minutes of oxygen plasma with parylene mostly removed
20 min: mostly removed
Slide after 25 minutes, parylene fully removed
25 min: fully removed

Test 2: higher pressure, 3× the oxygen flow

Recipe 2 (150 W, 15 sccm O₂, 205 mTorr) on the less uniform back side: the reading started at 123 and fell to 96 within the first 10 minutes, then to 76 and 69 against a 68 baseline after 15 and 20 minutes, with only isolated thick islands left. The emission reading tracked exactly what was seen on the glass — it can be trusted as the end-point signal.

Test 3

Restoring electrical contact on coated aluminum

A parylene-coated aluminum part was etched for 20 minutes per side with a similar recipe (150 W, 5 sccm O₂, 90 mTorr). Before etching, the surface resistance was beyond the meter's range; afterwards it read 0.3 Ω — the meter's lower limit. The thin-film interference colors visible before etching are gone afterwards.

That is the result failure analysts need: bare, conductive metal for probing, cross-sectioning or re-work, with no solvent residue.

Parylene coated aluminum part with rainbow interference colors before plasma etching
Before: coated, insulating
Aluminum part after oxygen plasma etching, parylene removed, bare metal
After 20 min: 0.3 Ω contact resistance
Takeaways

Parylene plasma removal in practice

End point you can read

Etch by-products raise the plasma emission; when it returns to the O₂ baseline the coating is gone. This works when the material underneath resists oxygen plasma (metal, glass, silicon, ceramics).

Coatings are rarely uniform

Thick spots, edges and the back side of a part clear last. Follow the emission reading instead of a fixed time.

Local or full removal

Plasma removes parylene everywhere it can reach. Mask areas you want to keep, or use it to strip whole boards and parts.

Recommended systems: Tergeo (150 W) for small parts; Tergeo-Plus and Tergeo-Pro (up to 500 W) for boards and batches. Related: polyimide ashing, plasma for failure analysis.

FAQ

Parylene removal questions

How fast does oxygen plasma remove parylene?

About 230 nm per minute in our test (150 W, 5 sccm O₂, 92 mTorr, direct mode) — a 4.7 µm coating clears in 20–25 minutes. Rate depends on power, pressure, part size and loading.

Will the plasma damage the circuit underneath?

Oxygen plasma does not etch metals, glass, ceramics or silicon, so it stops at the substrate. Other organic materials exposed to the plasma — solder mask, adhesives, plastic housings — will also be etched, so mask them if needed.

How do I know the parylene is completely removed?

Watch the plasma emission intensity on the Tergeo touchscreen. It rises while parylene is etching and returns to the pure-oxygen baseline when the coating is gone. A simple continuity or resistance check confirms it.

Not sure which plasma cleaner fits your process?

Tell us your samples, size and process gas. Our engineers reply within one to two business days with a recommendation and a quote.